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Preparation of Titanium Dioxide doped with Sulphur photocatalyst along with Nitrogen using Thiourea and Titanium Dioxide was performed in this work. The photocatalysts were prepared in the ratios of 1:3 and 1:4 with the former materials and the temperature effects were found out by varying the temperature of the photocatalysts prepared. The prepared photocatalysts were experimented on the staining dye named Basic Fuchsine for photodegradation using artificial light. The photodegradation was performed on the dye with various concentrations of the prepared photocatalysts.